N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine

Base Information

• Chemical Name: N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine
• CAS No.: 1444606-00-1
• Molecular Formula: C₄₂H₄₂N₄O₅S
• Molecular Weight: 714.885

Synonyms:N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine

Chemical Property of N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine

Chemical Property:

Purity/Quality:

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Technology Process of N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine

There total 4 articles about N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C42H41N4O5PolS → N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine (1444606-00-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.666667h; Wang resin Automated synthesizer;

DOI:10.1016/j.bmc.2012.09.053

Reference yield:

4-((((9H-fluoren-9-yl)methoxy)carbonyl)(4-methylthiobenzyl)amino)benzoic acid (1444605-66-6) → N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine (1444606-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / chloroform / 1 h / 20 °C

2: piperidine / N,N-dimethyl-formamide / 0.25 h

With piperidine; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In chloroform; N,N-dimethyl-formamide;

DOI:10.1002/anie.201410810

Reference yield:

4-((((9H-fluoren-9-yl)methoxy)carbonyl)(isobutyl)amino)benzoic acid (1233518-05-2) → N-(N-(N-(benzyl-4-aminobenzoyl)-N-4-methylthiobenzyl-4-aminobenzoyl)-N-isobutyl-4-aminobenzoyl)glycine (1444606-00-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / chloroform / 1 h / 20 °C

2: piperidine / N,N-dimethyl-formamide / 0.25 h

With piperidine; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; In chloroform; N,N-dimethyl-formamide;

DOI:10.1002/anie.201410810

upstream raw materials:

4-((((9H-fluoren-9-yl)methoxy)carbonyl)(4-methylthiobenzyl)amino)benzoic acid

4-((((9H-fluoren-9-yl)methoxy)carbonyl)(isobutyl)amino)benzoic acid

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