[(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane

Base Information

• Chemical Name: [(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane
• CAS No.: 1226976-41-5
• Molecular Formula: C₃₁H₄₅NO₈Si
• Molecular Weight: 587.786

Synonyms:[(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane

Chemical Property of [(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane

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Technology Process of [(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane

There total 1 articles about [(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H41NO7Si + benzoyl chloride (98-88-4) → [(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane (1226976-41-5)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2010.01.157

Reference yield: 97.0%

[(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane (1226976-41-5) → C25H31NO8 (1226976-44-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2010.01.157

Reference yield: 89.0%

[(2S,3S,4S,5S)-2-(3',4'-methylenedioxy)phenyl-3-methoxymethyleneoxy-4,5-isopropylidene-dioxy-6-tert-butyldimethylsilyloxy]-1-benzoylaminohexane (1226976-41-5) → C20H23NO7 (1226976-42-6)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2010.01.157

upstream raw materials:

benzoyl chloride

Downstream raw materials:

C₂₀H₂₃NO₇

C₂₅H₃₁NO₈

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