tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

Base Information

Chemical Name:tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate
CAS No.:1246523-39-6
Molecular Formula:C₂₁H₂₅Br₂NO₄
Molecular Weight:515.242
Hs Code.:

Synonyms:tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

Chemical Property:

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Technology Process of tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

There total 5 articles about tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₁₆H₁₇Br₂NO₂

: 1246523-43-2
tert-butyl 4-bromo-6-methoxy-3-(4-methoxyphenyl)indoline-1-carboxylate

: 1246523-39-6
tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 0.333333h;
DOI:10.1002/asia.201000544

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₁₆H₁₇Br₂NO₂

: 1246523-39-6
tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 0.333333h;
DOI:10.1002/anie.201001966

Reference yield:

: 1246523-40-9
1-(1-(2,6-dibromo-4-methoxyphenyl)-2-nitroethyl)-4-methoxybenzene

: 1246523-39-6
tert-butyl 2-(2,6-dibromo-4-methoxyphenyl)-2-(4-methoxyphenyl)ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; iron; iron(II) chloride / ethanol / 3.5 h / Reflux

2: triethylamine / acetonitrile / 0.33 h / 20 °C

With hydrogenchloride; iron; triethylamine; iron(II) chloride; In ethanol; acetonitrile;
DOI:10.1002/asia.201000544