C₂₅H₄₃NO₅Si

Base Information

Chemical Name:C₂₅H₄₃NO₅Si
CAS No.:1408058-31-0
Molecular Formula:C₂₅H₄₃NO₅Si
Molecular Weight:465.706
Hs Code.:

C<sub>25</sub>H<sub>43</sub>NO<sub>5</sub>Si

Synonyms:C₂₅H₄₃NO₅Si

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Chemical Property of C₂₅H₄₃NO₅Si

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Technology Process of C₂₅H₄₃NO₅Si

There total 14 articles about C₂₅H₄₃NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₄₁NO₄Si

: 108-24-7
acetic anhydride

: 1408058-31-0
C₂₅H₄₃NO₅Si

Guidance literature:: With pyridine; at 0 - 20 ℃; for 2h;
DOI:org/10.1016/j.tetlet.2012.08.143

Reference yield:

: 1393086-00-4
C₁₇H₂₂O₅

: 1408058-31-0
C₂₅H₄₃NO₅Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 2 h / 20 °C / Inert atmosphere

2.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 1 h / -15 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C

5.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

5.2: 4 h / 20 °C

6.1: pyridine / 2 h / 0 - 20 °C

With pyridine; 1H-imidazole; dmap; sodium azide; borane-THF; copper(II) bis(trifluoromethanesulfonate); triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 5.1: |Staudinger Azide Reduction / 5.2: |Staudinger Azide Reduction;
DOI:org/10.1016/j.tetlet.2012.08.143

Reference yield:

: 3458-28-4
D-Mannose

: 1408058-31-0
C₂₅H₄₃NO₅Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: sulfuric acid / N,N-dimethyl-formamide / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide

2.2: 4 h / 20 °C

3.1: hydrogenchloride; water / methanol / 4 h / 20 °C

4.1: sodium periodate / ethanol; water; methanol / 3 h / 20 °C

5.1: copper(II) bis(trifluoromethanesulfonate); borane-THF / 2 h / 20 °C / Inert atmosphere

6.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C / Inert atmosphere

7.1: pyridine / dichloromethane / 1 h / -15 °C / Inert atmosphere

8.1: sodium azide / N,N-dimethyl-formamide / 2 h / 20 °C

9.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

9.2: 4 h / 20 °C

10.1: pyridine / 2 h / 0 - 20 °C

With pyridine; 1H-imidazole; hydrogenchloride; dmap; sodium periodate; sodium azide; borane-THF; sulfuric acid; water; copper(II) bis(trifluoromethanesulfonate); sodium hydride; triphenylphosphine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; 9.1: |Staudinger Azide Reduction / 9.2: |Staudinger Azide Reduction;
DOI:org/10.1016/j.tetlet.2012.08.143