Bn₂-L-Hpg(Tf)-OBn

Base Information

Chemical Name:Bn₂-L-Hpg(Tf)-OBn
CAS No.:1352788-61-4
Molecular Formula:C₃₀H₂₆F₃NO₅S
Molecular Weight:569.601
Hs Code.:

Synonyms:Bn₂-L-Hpg(Tf)-OBn

Suppliers and Price of Bn₂-L-Hpg(Tf)-OBn

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bn₂-L-Hpg(Tf)-OBn

Chemical Property:

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Technology Process of Bn₂-L-Hpg(Tf)-OBn

There total 5 articles about Bn₂-L-Hpg(Tf)-OBn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₄F₃NO₅S

: 100-39-0
benzyl bromide

: 1352788-61-4
Bn₂-L-Hpg(Tf)-OBn

Guidance literature:: With sodium hydrogencarbonate; In dimethyl sulfoxide; at 25 ℃; for 25h;
DOI:10.1002/anie.201103315

Reference yield:

: 1352788-60-3
Cbz-L-Hpg(Tf)-OBn

: 1352788-61-4
Bn₂-L-Hpg(Tf)-OBn

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylsulfide; trifluoroacetic acid / 17 h / 25 °C

2: sodium hydrogencarbonate / dimethyl sulfoxide / 25 h / 25 °C

With dimethylsulfide; sodium hydrogencarbonate; trifluoroacetic acid; In dimethyl sulfoxide;
DOI:10.1002/anie.201103315

Reference yield:

: 32462-30-9
(S)-hydroxyphenylglycine

: 1352788-61-4
Bn₂-L-Hpg(Tf)-OBn

Guidance literature:: Multi-step reaction with 5 steps

1: sodium carbonate / 1,4-dioxane; water / 1.5 h / 0 - 25 °C

2: sodium hydrogencarbonate / N,N-dimethyl-formamide / 15 h / 25 °C

3: pyridine / dichloromethane / 0.58 h / 0 - 25 °C

4: dimethylsulfide; trifluoroacetic acid / 17 h / 25 °C

5: sodium hydrogencarbonate / dimethyl sulfoxide / 25 h / 25 °C

With pyridine; dimethylsulfide; sodium hydrogencarbonate; sodium carbonate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/anie.201103315