(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Base Information

Chemical Name:(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid
CAS No.:152871-72-2
Molecular Formula:C₂₈H₃₀N₂O₉S
Molecular Weight:570.62
Hs Code.:

Synonyms:(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

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Chemical Property of (R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

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Technology Process of (R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

There total 3 articles about (R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 152871-69-7
(R)-2-Amino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

: 152871-72-2
(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Guidance literature:: With sodium hydrogencarbonate; In water; acetone; for 12h; Ambient temperature;

Reference yield:

: 146548-59-6
2,4,6-trimethoxy benzyl amine hydrochloride

: 152871-72-2
(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DIPEA / dimethylformamide / 1 h / 0 °C

2: 82 percent / hydrogen / Pd/C / methanol

3: 85 percent / NaHCO₃ / acetone; H₂O / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 152871-65-3
(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

: 152871-72-2
(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / hydrogen / Pd/C / methanol

2: 85 percent / NaHCO₃ / acetone; H₂O / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; water; acetone;