(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Base Information

Chemical Name:(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid
CAS No.:152871-65-3
Molecular Formula:C₂₁H₂₆N₂O₉S
Molecular Weight:482.511
Hs Code.:

Synonyms:(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

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Chemical Property of (R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

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Technology Process of (R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

There total 1 articles about (R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 64957-08-0
2-benzyloxycarbonylamino-3-chlorosulfonylpropionic acid benzyl ester

: 146548-59-6
2,4,6-trimethoxy benzyl amine hydrochloride

: 152871-65-3
(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

: 152871-64-2
(S)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid benzyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

Reference yield: 82.0%

: 152871-65-3
(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

: 152871-69-7
(R)-2-Amino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;

Reference yield:

: 152871-65-3
(R)-2-Benzyloxycarbonylamino-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

: 152871-72-2
(R)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-(2,4,6-trimethoxy-benzylsulfamoyl)-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / hydrogen / Pd/C / methanol

2: 85 percent / NaHCO₃ / acetone; H₂O / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; water; acetone;