2,4,6-TRIS(3,5-DIMETHYLPHENYL)BOROXIN

Base Information

• Chemical Name: 2,4,6-TRIS(3,5-DIMETHYLPHENYL)BOROXIN
• CAS No.: 34907-38-5
• Molecular Formula: C24H27 B3 O3
• Molecular Weight: 395.91
• Hs Code.: 2934999090
• Mol file: 34907-38-5.mol

Synonyms:Boroxin,tris(3,5-dimethylphenyl)- (9CI)

Chemical Property of 2,4,6-TRIS(3,5-DIMETHYLPHENYL)BOROXIN

Chemical Property:

• PSA: 27.69000
• LogP: 3.08640

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6-TRIS(3,5-DIMETHYLPHENYL)BOROXIN

There total 7 articles about 2,4,6-TRIS(3,5-DIMETHYLPHENYL)BOROXIN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethylphenyl boronic acid (172975-69-8) + phenylboronic acid (98-80-6) → triphenylboroxine (3262-89-3) + C20H19B3O3 + C22H23B3O3 + tris(3.5-dimethyl phenyl)boroxine (34907-38-5)

Guidance literature:

With water; at 25 ℃;

Reference yield:

3,5-dimethylphenyl boronic acid (172975-69-8) → tris(3.5-dimethyl phenyl)boroxine (34907-38-5)

Guidance literature:

In toluene; Reflux; Inert atmosphere;

DOI:10.1021/ol9029534

Reference yield:

Trimethyl borate (121-43-7,63156-11-6) + 3,5-dimethyphenylmagnesium bromide (34696-73-6) → tris(3.5-dimethyl phenyl)boroxine (34907-38-5)

Guidance literature:

With sulfuric acid; water; byproducts: H2O; dehydration with petroleum ether;;

upstream raw materials:

(4-methoxy-3,5-dimethylphenyl)boronic acid

3,5-dimethylphenyl boronic acid

3,4,5-trimethoxyphenylboronic Acid

4-methoxy-3,5-di-tert-butylphenylboronic acid pinacol ester

Downstream raw materials:

3,5-dimethylphenyl boronic acid

C₁₆H₁₈O

B₃O₃(CH₃C₆H₃CH₃)3(CH₃NH₂)

tri(3,5-dimethylphenyl)boroxine, morpholine adduct