(3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid

Base Information Edit

Chemical Name:(3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid
CAS No.:233584-42-4
Molecular Formula:C₁₅H₂₅BO₃
Molecular Weight:264.173
Hs Code.:
Nikkaji Number:J1.178.427E
Mol file:233584-42-4.mol

Synonyms:(3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid;233584-42-4;(3,5-ditert-butyl-4-methoxyphenyl)boronic acid;Boronic acid, [3,5-bis(1,1-dimethylethyl)-4-methoxyphenyl]-;C15H25BO3;3,5-Di-tert-butyl-4-methoxy-phenylboronic acid;(3,5-Di-tert-butyl-4-methoxyphenyl)boronic acidE;(3,5-DI-TERT-BUTYL-4-METHOXYPHENYL) BORONIC ACID

Suppliers and Price of (3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of (3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid Edit

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:264.1896748
Heavy Atom Count:19
Complexity:267

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:B(C1=CC(=C(C(=C1)C(C)(C)C)OC)C(C)(C)C)(O)O

Technology Process of (3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid

There total 11 articles about (3,5-Di-tert-butyl-4-methoxyphenyl)boronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1516-96-7
4-bromo-2,6-di-tert-butylanisole

: 233584-42-4
4-methoxy-3,5-di-tert-butylphenylboronic acid pinacol ester

Guidance literature:: 4-bromo-2,6-di-tert-butylanisole; With tert.-butyl lithium; In tetrahydrofuran; n-heptane; at -78 ℃; for 2h; Inert atmosphere;

With Triisopropyl borate; In tetrahydrofuran; n-heptane; for 0.25h; Inert atmosphere;
DOI:10.1002/chem.201805655

Reference yield: 58.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 1516-96-7
4-bromo-2,6-di-tert-butylanisole

: 7732-18-5
water

: 233584-42-4
4-methoxy-3,5-di-tert-butylphenylboronic acid pinacol ester

Guidance literature:: 4-bromo-2,6-di-tert-butylanisole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

water; With sodium hydroxide; In diethyl ether; Inert atmosphere;
DOI:10.1002/ejic.201900716