N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

Base Information

Chemical Name:N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide
CAS No.:160580-61-0
Molecular Formula:C₂₃H₃₄N₂O₃Si
Molecular Weight:414.62
Hs Code.:

Synonyms:N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

Chemical Property:

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Technology Process of N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

There total 8 articles about N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 160580-60-9
N-<7-tert-butyldimethylsiloxy)-6-(3-nitrophenyl)hept-3-ynyl>succinimide

: 160580-61-0
N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

Guidance literature:: With iron; acetic acid; In ethanol; for 2h; Heating;

Reference yield:

: 10268-12-9
methyl 3-nitrophenylacetate

: 160580-61-0
N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

Guidance literature:: Multi-step reaction with 6 steps

1: 76 percent / LDA / hexane; tetrahydrofuran / -78 °C

2: 89 percent / LiAlH₄ / tetrahydrofuran / -78 - -40 °C

3: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

4: 28 percent / LDA

5: 91 percent / DEAD, Ph₃P / tetrahydrofuran / 3 h / Ambient temperature

6: 82 percent / Fe, AcOH / ethanol / 2 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; iron; acetic acid; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; ethanol; hexane; N,N-dimethyl-formamide;

Reference yield:

: 1877-73-2
3-nitro-benzeneacetic acid

: 160580-61-0
N-<6-(3-aminophenyl)-7-(tert-butyldimethylsiloxy)hept-3-ynyl>succinimide

Guidance literature:: Multi-step reaction with 7 steps

1: 94 percent / H₂SO₄ / 2.5 h / Heating

2: 76 percent / LDA / hexane; tetrahydrofuran / -78 °C

3: 89 percent / LiAlH₄ / tetrahydrofuran / -78 - -40 °C

4: 98 percent / imidazole / dimethylformamide / 16 h / Ambient temperature

5: 28 percent / LDA

6: 91 percent / DEAD, Ph₃P / tetrahydrofuran / 3 h / Ambient temperature

7: 82 percent / Fe, AcOH / ethanol / 2 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; sulfuric acid; iron; acetic acid; triphenylphosphine; lithium diisopropyl amide; diethylazodicarboxylate; In tetrahydrofuran; ethanol; hexane; N,N-dimethyl-formamide;