N-chloro-p-chlorobenzenesulfonamide sodium salt

Base Information

• Chemical Name: N-chloro-p-chlorobenzenesulfonamide sodium salt
• CAS No.: 30066-82-1
• Molecular Formula: C₆H₄Cl₂NNaO₂S
• Molecular Weight: 248.065
• Mol file: 30066-82-1.mol

Synonyms:N-chloro-p-chlorobenzenesulfonamide sodium salt

Chemical Property of N-chloro-p-chlorobenzenesulfonamide sodium salt

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-chloro-p-chlorobenzenesulfonamide sodium salt

There total 2 articles about N-chloro-p-chlorobenzenesulfonamide sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

N,N-dichloro-4-chlorobenzenesulfonamide (17260-65-0) → N-chloro-p-chlorobenzenesulfonamide sodium salt (30066-82-1)

Guidance literature:

With sodium hydroxide; In water;

Reference yield:

→ N-chloro-p-chlorobenzenesulfonamide sodium salt (30066-82-1)

Guidance literature:

/BRN= 417525/, NaOH;

DOI:10.1055/s-1976-24176

Reference yield: 92.0%

2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane (16892-64-1) + N-chloro-p-chlorobenzenesulfonamide sodium salt (30066-82-1) → CH3OSn(CH3)2S(NSO2C6H4Cl)Sn(CH3)2SSn(CH3)2NHSO2C6H4Cl (206008-10-8) + sulfur (7704-34-9) + sodium chloride (7647-14-5)

Guidance literature:

In methanol; soln. of N-compd. addn. to soln. of Sn compd. (vacuum, stirring), heating (50°C, 30 min); mixture cooling (ice bath), ppt. filtration off and extracting with water to remove NaCl and with acetone to remove S, alcoholic filtrate vacuumevapn., residue treating with diethyl ether, soln. decanting and vacuum evapn.; elem. anal.;

upstream raw materials:

N,N-dichloro-4-chlorobenzenesulfonamide

Downstream raw materials:

N-Chlor-N-(2-hydroxyaethyl)-p-chlorbenzolsulfonamid

C₁₃H₁₂Cl₂N₂O₄S₃

1.1.1.3-Tetrachlor-2-(N-p-chlorbenzolsulfonamid)-propan

C₁₅H₁₃Cl₅N₂O₄S₂

Refernces