RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

Base Information

Chemical Name:RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)
CAS No.:78295-09-7
Molecular Formula:C₄₉H₅₄ClOP₂Rh
Molecular Weight:859.273
Hs Code.:

RhCl(P(C<sub>6</sub>H<sub>4</sub>(CH<sub>2</sub>CH<sub>3</sub>))3)2(CO)

Synonyms:RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

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Chemical Property of RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

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Technology Process of RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

There total 1 articles about RhCl(P(C₆H₄(CH₂CH₃))3)2(CO) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: di(rhodium)tetracarbonyl dichloride

: 50777-22-5
tris(p-ethylphenyl)phosphine

: 78295-09-7
RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

Guidance literature:: In chloroform; byproducts: CO; method of Mague and Mitchener, Inorg.Chem., 8, 119 (1969); recrystn. (EtOH/CHCl3); elem. anal.;
DOI:10.1016/S0020-1693(00)89336-6

Reference yield: 89.0%

: 78295-09-7
RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

: [Rh₂I₂(P(p-EtC₆H₄)3)4]

Guidance literature:: With potassium iodide; In acetone; byproducts: KCl, KI; addn. of KI in acetone to complex, stirred 3h, KI and KCl filtered off,evapn. under reduced press., residue dissolved in CHCl3, filtered, evapn. to dryness, washed with ethanol, dried; elem. anal.; identified by chromy.;
DOI:10.1016/0022-328X(83)85124-9

Reference yield: 56.0%

: 78295-09-7
RhCl(P(C₆H₄(CH₂CH₃))3)2(CO)

: 7647-15-6
sodium bromide

: 87552-34-9
RhBr(CO)(P((C₆H₄)C₂H₅)3)2

Guidance literature:: In acetone; byproducts: NaCl; addn. of NaBr in actone to complex, stirred 2,5h, room temp., filtered,evapn. of solvent under reduced press., residue washed with EtOH, filtered, dried; on air; recrystn. from benzene/EtOH; elem. anal., chromy.;
DOI:10.1016/0022-328X(83)85124-9