C₁₅H₂₉N₂O₅P

Base Information

Chemical Name:C₁₅H₂₉N₂O₅P
CAS No.:1122748-00-8
Molecular Formula:C₁₅H₂₉N₂O₅P
Molecular Weight:348.379
Hs Code.:

C<sub>15</sub>H<sub>29</sub>N<sub>2</sub>O<sub>5</sub>P

Synonyms:C₁₅H₂₉N₂O₅P

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Chemical Property of C₁₅H₂₉N₂O₅P

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Technology Process of C₁₅H₂₉N₂O₅P

There total 28 articles about C₁₅H₂₉N₂O₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 950478-34-9
diethyl (3R,4R,5S)-4-acetamido-5-amino-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate

: 1122748-00-8
C₁₅H₂₉N₂O₅P

Guidance literature:: With sodium ethanolate; In ethanol; at 25 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm3008486

Reference yield:

: 1062100-87-1
diethyl (3R,4R,5S)-4-acetamido-5-tert-butoxycarbonylamino-3-(1-ethylpropoxy)cyclohex-1-ene-1-phosphonate

: 1122748-00-8
C₁₅H₂₉N₂O₅P

Guidance literature:: diethyl (3R,4R,5S)-4-acetamido-5-tert-butoxycarbonylamino-3-(1-ethylpropoxy)cyclohex-1-ene-1-phosphonate; With sodium ethanolate; In ethanol; at 20 ℃; for 16h;

With Amberlite IR-120; In ethanol; at 40 ℃; for 2h;

Reference yield:

: C₈H₁₅NO₄

: 1122748-00-8
C₁₅H₂₉N₂O₅P

Guidance literature:: Multi-step reaction with 14 steps

1: pyridine / 3 h / 25 °C

2: hydrogenchloride / 1,4-dioxane; toluene; water / 24 h / 0 - 25 °C

3: toluene-4-sulfonic acid / toluene / 4 h / 80 °C

4: pyridine / dichloromethane / 2 h / -15 °C

5: sodium hydride; 15-crown-5 / N,N-dimethyl-formamide / 24 h / 25 °C

6: hydrogen; palladium on activated charcoal / ethanol / 24 h / 25 °C

7: sodium ethanolate / ethanol / 5 h / 25 °C

8: diphenyl phosphoryl azide; diisopropyl-carbodiimide; triphenylphosphine / tetrahydrofuran / 48 h / 25 °C

9: hydrogenchloride / ethanol / 1 h / Reflux

10: pyridine / dichloromethane / 2 h / -15 - -10 °C

11: potassium nitrite; 18-crown-6 ether / N,N-dimethyl-formamide / 24 h / 40 °C

12: trifluorormethanesulfonic acid / dichloromethane / 24 h / 25 °C

13: hydrogen / ethanol / 16 h / 25 °C

14: sodium ethanolate / ethanol / 16 h / 25 °C / Inert atmosphere

With pyridine; hydrogenchloride; potassium nitrite; 15-crown-5; 18-crown-6 ether; trifluorormethanesulfonic acid; diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; sodium ethanolate; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; diisopropyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm3008486