N,N-DIBOC-2-CHLORO-4-AMINOANILINE

Base Information Edit

Chemical Name:N,N-DIBOC-2-CHLORO-4-AMINOANILINE
CAS No.:252019-51-5
Molecular Formula:C16H23 Cl N2 O4
Molecular Weight:342.823
Hs Code.:
Mol file:252019-51-5.mol

Synonyms:Imidodicarbonicacid, (4-amino-2-chlorophenyl)-, bis(1,1-dimethylethyl) ester (9CI); tert-Butyl2-(tert-butoxycarbonyl)-2-(4-amino-2-chlorophenyl)carbamate

Suppliers and Price of N,N-DIBOC-2-CHLORO-4-AMINOANILINE

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-1,N-1-BIS-(TERT-BUTOXYCARBONYL)-2-CHLORO-PARA-PHENYLENEDIAMINE 95.00%
5MG
$ 504.86

AccelPharmtech
2-(4-amino-2-chlorophenyl)-Imidodicarbonicacid,1,3-bis(1,1-dimethylethyl)ester 97.00%
25G
$ 4010.00

AccelPharmtech
2-(4-amino-2-chlorophenyl)-Imidodicarbonicacid,1,3-bis(1,1-dimethylethyl)ester 97.00%
5G
$ 2180.00

Total 1 raw suppliers

Chemical Property of N,N-DIBOC-2-CHLORO-4-AMINOANILINE Edit

Chemical Property:

Boiling Point:437.8±55.0 °C(Predicted)
PKA:3.09±0.10(Predicted)
PSA：81.86000
Density:1.220±0.06 g/cm3(Predicted)
LogP:5.18000

Purity/Quality:

98%min ^*data from raw suppliers

N-1,N-1-BIS-(TERT-BUTOXYCARBONYL)-2-CHLORO-PARA-PHENYLENEDIAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N,N-DIBOC-2-CHLORO-4-AMINOANILINE

There total 5 articles about N,N-DIBOC-2-CHLORO-4-AMINOANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 252019-65-1
tert-butyl N-[(tert-butoxy)carbonyl]-N-(2-chloro-4-nitrophenyl)carbamate

: 252019-51-5
N¹,N¹-bis(tert-butoxycarbonyl)-2-chloro-p-phenylenediamine

Guidance literature:: With iron; acetic acid; In methanol; for 0.5h; Heating;
DOI:10.1021/jm040159c

Reference yield: 93.0%

: 252019-51-5
N¹,N¹-bis(tert-butoxycarbonyl)-2-chloro-p-phenylenediamine

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethyl acetate; at 20 - 24 ℃;

Reference yield:

: 121-87-9
2-Chloro-4-nitroaniline

: 252019-51-5
N¹,N¹-bis(tert-butoxycarbonyl)-2-chloro-p-phenylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / DMAP / tetrahydrofuran / 3 h / 25 °C

2: 100 percent / iron; AcOH / methanol / 0.5 h / Heating

With dmap; iron; acetic acid; In tetrahydrofuran; methanol;
DOI:10.1021/jm040159c