(2E)-1-(4-Nitrophenyl)-2-[(2-nitrophenyl)methylidene]hydrazine

Base Information

• Chemical Name: (2E)-1-(4-Nitrophenyl)-2-[(2-nitrophenyl)methylidene]hydrazine
• CAS No.: 7510-47-6
• Molecular Formula: C13H10 N4 O4
• Molecular Weight: 286.247
• DSSTox Substance ID: DTXSID00422122

Synonyms:DTXSID00422122;7510-47-6;AKOS003408910;2-Nitrobenzaldehyde 4-nitrophenylhydrazone;(E)-2-Nitrobenzaldehyde 4-nitrophenylhydrazone;1-(2-nitrobenzylidene)-2-(4-nitrophenyl)hydrazine;(2E)-1-(4-Nitrophenyl)-2-[(2-nitrophenyl)methylidene]hydrazine

Chemical Property of (2E)-1-(4-Nitrophenyl)-2-[(2-nitrophenyl)methylidene]hydrazine

Chemical Property:

• Vapor Pressure: 1.06E-09mmHg at 25°C
• Boiling Point: 488.7°Cat760mmHg
• Flash Point: 249.4°C
• Density: 1.39g/cm³
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 3
• Exact Mass: 286.07020481
• Heavy Atom Count: 21
• Complexity: 396

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C=NNC2=CC=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]
• Isomeric SMILES: C1=CC=C(C(=C1)/C=N/NC2=CC=C(C=C2)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of (2E)-1-(4-Nitrophenyl)-2-[(2-nitrophenyl)methylidene]hydrazine

There total 2 articles about (2E)-1-(4-Nitrophenyl)-2-[(2-nitrophenyl)methylidene]hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrophenylhydrazone (100-16-3) + 2-nitro-benzaldehyde (552-89-6) → 2-nitro-benzaldehyde (4-nitro-phenyl)-hydrazone (7510-47-6)

Guidance literature:

With acetic acid;

Reference yield:

→ 2-nitro-benzaldehyde (4-nitro-phenyl)-hydrazone (7510-47-6)

Guidance literature:

2-Nitro-benzaldehyd, 4-Nitro-phenylhydrazin/Eg.;

DOI:10.1039/j29660001031

Reference yield: 65.0%

2-nitro-benzaldehyde (4-nitro-phenyl)-hydrazone (7510-47-6) → 2-nitro-benzaldehyde (552-89-6)

Guidance literature:

With <(Py)2Ag>2Cr2O7; In benzene; for 10h; Heating;

upstream raw materials:

4-nitrophenylhydrazone

2-nitro-benzaldehyde

Downstream raw materials:

3-(4-nitro-phenylazo)-benzo[c]isoxazole 1-oxide

2-nitro-benzaldehyde

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