Pyrazino[2,3-b]pyrazine, decahydro-4a,8a-dimethyl-, cis- (9CI)

Base Information

• Chemical Name: Pyrazino[2,3-b]pyrazine, decahydro-4a,8a-dimethyl-, cis- (9CI)
• CAS No.: 252010-70-1
• Molecular Formula: C₈H₁₈N₄
• Molecular Weight: 170.258
• Mol file: 252010-70-1.mol

Synonyms:Pyrazino[2,3-b]pyrazine, decahydro-4a,8a-dimethyl-, cis- (9CI);CIS-4A,8A-DIMETHYLDECAHYDROPYRAZINO[2,3-B]PYRAZINE

Chemical Property of Pyrazino[2,3-b]pyrazine, decahydro-4a,8a-dimethyl-, cis- (9CI)

Chemical Property:

• PSA: 48.12000
• LogP: 0.11960

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Pyrazino[2,3-b]pyrazine, decahydro-4a,8a-dimethyl-, cis- (9CI)

There total 3 articles about Pyrazino[2,3-b]pyrazine, decahydro-4a,8a-dimethyl-, cis- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.6%

5,6-dimethyl-2,3-dihydropyrazine (15986-92-2) + ethylenediamine (107-15-3,85404-18-8) → cis-4a,8a-dimethyltetraazadecalin (252010-70-1)

Guidance literature:

at 20 ℃;

DOI:10.3987/COM-99-8678

Reference yield: 41.5%

5,6-dimethyl-2,3-dihydropyrazine (15986-92-2) + trans-1,2-Diaminocyclohexane (1121-22-8,1436-59-5,20439-47-8,21436-03-3,41013-43-8,694-83-7) → cis-4a,8a-dimethyltetraazadecalin (252010-70-1) + trans-2,3-trans-6,7-bis(tetramethylene)-cis-4a,8a-dimethyl-1,4,5,8-tetraazadecalin

Guidance literature:

In acetonitrile; Product distribution;

DOI:10.3987/COM-00-8932

Reference yield:

1,2-ethanediamine monohydrate (6780-13-8,16889-59-1) + dimethylglyoxal (431-03-8) → 4a,8a-dimethyl-decahydro-pyrazino[2,3-b]pyrazine (75804-30-7,252010-70-1)

Guidance literature:

With benzene;

upstream raw materials:

1,2-ethanediamine monohydrate

dimethylglyoxal

5,6-dimethyl-2,3-dihydropyrazine

ethylenediamine

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