N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

Base Information

Chemical Name:N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid
CAS No.:173375-30-9
Molecular Formula:C₁₅H₁₅N₃O₅
Molecular Weight:317.301
Hs Code.:

Synonyms:N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

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Chemical Property of N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

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Technology Process of N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

There total 5 articles about N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 108-30-5
succinic acid anhydride

: 173375-23-0
4-(4-Aminobenzoyl)-1,3-dihydro-5-methyl-3H-imidazol-2-one

: 173375-30-9
N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

Guidance literature:: With pyridine; dmap; for 2h; Ambient temperature;
DOI:10.1002/ardp.19953281005

Reference yield:

: 5383-83-5
4–(1,3-dioxoisoindolin-2-yl)benzoyl chloride

: 173375-30-9
N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / AlCl₃ / nitrobenzene / 6 h / 60 °C

2: 85 percent / 1 M aq. Na₂CO₃, hydrazine hydrate / 10 h / Ambient temperature

3: 95 percent / DMAP, pyridine / 2 h / Ambient temperature

With pyridine; dmap; aluminium trichloride; sodium carbonate; hydrazine hydrate; In nitrobenzene;
DOI:10.1002/ardp.19953281005

Reference yield:

: 173375-29-6
N-<4-<(1,3-Dihydro-5-methyl-2-oxo-3H-imidazol-4-yl)carbonyl>phenyl>-4-phthalimidobutanamide

: 173375-30-9
N-[4-(5-Methyl-2-oxo-2,3-dihydro-1H-imidazole-4-carbonyl)-phenyl]-succinamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / 1 M aq. Na₂CO₃, hydrazine hydrate / 24 h / Ambient temperature

2: 1.) MeCN, r.t., 2.) reflux, 20 h

3: 1 M aq. HCl

4: 95 percent / DMAP, pyridine / 2 h / Ambient temperature

With pyridine; hydrogenchloride; dmap; sodium carbonate; hydrazine hydrate;
DOI:10.1002/ardp.19953281005