2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

Base Information

Chemical Name:2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile
CAS No.:154458-80-7
Molecular Formula:C₃₃H₂₇N₃O₆
Molecular Weight:561.594
Hs Code.:

Synonyms:2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

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Technology Process of 2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

There total 1 articles about 2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68423-37-0
2-Nitro-5-(benzyloxy)-benzylchlorid

: 50299-95-1,35096-40-3
2-benzoyl-1-cyano-6,7-dimethoxy-1,2-dihydroisoquinoline

: 154458-80-7
2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

Guidance literature:: With sodium hydroxide; water; benzyltrimethylammonium chloride; Yield given. Multistep reaction; 1.) benzene, 10 min, 2.) benzene, water, RT, 90 min;

Reference yield: 72.0%

: 154458-80-7
2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

: 154458-81-8
1-<2-nitro-5-benzyloxybenzyl>-6,7-dimethoxyisoquinoline

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In N,N-dimethyl-formamide; for 0.75h;

Reference yield:

: 154458-80-7
2-benzoyl-1-<5-benzyloxy-2-nitrobenzyl>-1,2-dihydro-6,7-dimethoxyisoquinaldonitrile

: 154458-82-9
4-amino-α-(6,7-dimethoxy-1-isoquinolinyl)-m-cresol

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Triton B / dimethylformamide / 0.75 h

2: 43 percent / H₂, K₂CO₃ / 5percent Pd/C / aq. ethanol / 3 h / 2947.7 Torr

With hydrogen; N-benzyl-trimethylammonium hydroxide; potassium carbonate; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;