(Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

Base Information

Chemical Name:(Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide
CAS No.:1312764-81-0
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:

Synonyms:(Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

Suppliers and Price of (Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

There total 2 articles about (Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 16649-50-6
N-tert-Butylhydroxylamine

: 112579-47-2
5-acetyl-2-hydroxy-3-methoxybenzaldehyde

: 1312764-81-0
(Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

Guidance literature:: In methanol; for 6h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2011.03.056

Reference yield:

: 498-02-2
1-(3-methoxy-4-hydroxyphenyl)ethanone

: 1312764-81-0
(Z)-N-(5-acetyl-2-hydroxy-3-methoxybenzylidene)-2-methylpropan-2-amine oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; sodium hydroxide / ethanol / 2 h / 70 °C

1.2: pH 1

2.1: methanol / 6 h / Inert atmosphere; Reflux

With triethylamine; sodium hydroxide; In methanol; ethanol; 1.1: Reimer-Tiemann reaction;
DOI:10.1016/j.ejmech.2011.03.056