N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide

Base Information

Chemical Name:N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide
CAS No.:1421663-40-2
Molecular Formula:C₂₇H₃₀BN₃O₄
Molecular Weight:471.364
Hs Code.:

Synonyms:N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide

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Chemical Property of N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide

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Technology Process of N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide

There total 2 articles about N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 54-85-3,7640-37-1
isoniazid

: 1421663-44-6
1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethanone

: 1421663-40-2
N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide

Guidance literature:: In N,N-dimethyl-formamide; toluene; for 32h; Reflux;

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 138500-85-3
4-bromomethylphenylboronic acid pinacol ester

: 1421663-40-2
N'-(1-(2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyloxy)phenyl)ethylidene)isonitotinohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 110 °C

2: N,N-dimethyl-formamide; toluene / 32 h / Reflux

With potassium carbonate; In N,N-dimethyl-formamide; toluene;