1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Base Information

• Chemical Name: 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione
• CAS No.: 194672-76-9
• Molecular Formula: C₃₅H₄₂N₂O₇SeSi
• Molecular Weight: 709.773

Synonyms:1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Chemical Property of 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione

There total 3 articles about 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylselenyl chloride (5707-04-0) + 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-3-O-(methoxyethoxymethylene)-D-erythro-pent-1-enitol (161758-89-0) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-5-phenylselanyl-1H-pyrimidine-2,4-dione + 1-[(2S,3S,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2S,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione (194672-76-9)

Guidance literature:

With silver trifluoromethanesulfonate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; 1.) ether, room temperature, 5 min, 2.) ether, room temperature, 1 h;

DOI:10.1016/S0040-4020(97)00697-2

Reference yield:

Phenylselenyl chloride (5707-04-0) + 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-3-O-(methoxyethoxymethylene)-D-erythro-pent-1-enitol (161758-89-0) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-5-phenylselanyl-1H-pyrimidine-2,4-dione + 1-[(2R,3S,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2S,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione (194672-76-9)

Guidance literature:

With silver trifluoromethanesulfonate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; 1.) ether, room temperature, 5 min, 2.) ether, room temperature, 1 h;

DOI:10.1016/S0040-4020(97)00697-2

Reference yield:

Phenylselenyl chloride (5707-04-0) + 1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-3-O-(methoxyethoxymethylene)-D-erythro-pent-1-enitol (161758-89-0) + O,O'-bis-(trimethylsilyl)uracil (10457-14-4) → 1-[(2S,3S,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2R,3S,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2S,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione + 1-[(2R,3R,4R,5R)-5-(tert-Butyl-diphenyl-silanyloxymethyl)-4-(2-methoxy-ethoxymethoxy)-3-phenylselanyl-tetrahydro-furan-2-yl]-1H-pyrimidine-2,4-dione (194672-76-9)

Guidance literature:

With silver trifluoromethanesulfonate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given; 1.) ether, room temperature, 5 min, 2.) ether, room temperature, 1 h;

DOI:10.1016/S0040-4020(97)00697-2

upstream raw materials:

Phenylselenyl chloride

1,4-anhydro-5-O-(tert-butyldiphenylsilyl)-2-deoxy-3-O-(methoxyethoxymethylene)-D-erythro-pent-1-enitol

O,O'-bis-(trimethylsilyl)uracil

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