(E)-3-Phenyl-1-(4-[(E)-(3-phenyl-acryloyl)]-phenyl)-propenone

Base Information

• Chemical Name: (E)-3-Phenyl-1-(4-[(E)-(3-phenyl-acryloyl)]-phenyl)-propenone
• CAS No.: 34838-64-7
• Molecular Formula: C24H18 O2
• Molecular Weight: 338.406
• Mol file: 34838-64-7.mol

Synonyms:(E)-3-Phenyl-1-(4-[(E)-(3-phenyl-acryloyl)]-phenyl)-propenone

Chemical Property of (E)-3-Phenyl-1-(4-[(E)-(3-phenyl-acryloyl)]-phenyl)-propenone

Chemical Property:

• Boiling Point: 544.6°Cat760mmHg
• Flash Point: 199.8°C
• PSA: 34.14000
• Density: 1.166g/cm³
• LogP: 5.47880

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (E)-3-Phenyl-1-(4-[(E)-(3-phenyl-acryloyl)]-phenyl)-propenone

There total 6 articles about (E)-3-Phenyl-1-(4-[(E)-(3-phenyl-acryloyl)]-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1,4-Diacetylbenzene (1009-61-6) + benzaldehyde (100-52-7) → (2E,2′E)-1,1′-(1,4-phenylene)bis(3-phenylprop-2-en-1-one) (34838-64-7)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 20 ℃; for 0.3h;

DOI:10.1007/s00044-011-9696-z

Reference yield: 83.0%

4-ethynylacetophenone (42472-69-5) + benzaldehyde (100-52-7) → (2E,2′E)-1,1′-(1,4-phenylene)bis(3-phenylprop-2-en-1-one) (34838-64-7)

Guidance literature:

With phosphonic Acid; In hexane; water; at 110 ℃; for 36h; Schlenk technique; Green chemistry;

DOI:10.1055/s-0035-1560832

Reference yield: 80.0%

1,4-diethynylbenzene (935-14-8) + benzaldehyde (100-52-7) → (2E,2′E)-1,1′-(1,4-phenylene)bis(3-phenylprop-2-en-1-one) (34838-64-7)

Guidance literature:

With phosphonic Acid; In hexane; water; at 110 ℃; for 36h; Schlenk technique; Green chemistry;

DOI:10.1055/s-0035-1560832

upstream raw materials:

1,4-Diacetylbenzene

benzaldehyde

benzene-1,4-diyl diacetate

p-Terephthaloyl-bis-methylen-triphenylphosphoran

Downstream raw materials:

1,1'-terephthaloylbis<2-phenyl-3-(phenylsulfonyl)cyclopropane>

1,1'-terephthaloylbis<2-phenyl-3-(phenylthio)cyclopropane>

[4-(4-Phenyl-4,5-dihydro-1H-pyrazole-3-carbonyl)-phenyl]-(4-phenyl-4,5-dihydro-1H-pyrazol-3-yl)-methanone

C₁₄₄H₁₀₈O₁₂