1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat

Base Information

• Chemical Name: 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat
• CAS No.: 24707-07-1
• Molecular Formula: C₃₄H₄₆O₆
• Molecular Weight: 550.736
• Mol file: 24707-07-1.mol

Synonyms:1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat

Chemical Property of 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat

There total 4 articles about 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Bicyclo<2.2.2.>octan-1,4-dicarbonsauere-ethylester (1659-75-2) → 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat (24707-07-1)

Guidance literature:

Multi-step reaction with 4 steps

1: KOH / ethanol

2: Br₂, HgO, BrCH₂CH₂Br

3: CuO, Fe / 215 °C

4: Py

With pyridine; potassium hydroxide; bromine; iron; ethylene dibromide; copper(II) oxide; mercury(II) oxide; In ethanol;

DOI:10.1021/ja00709a026

Reference yield:

1,4-bicyclo[2.2.2]octanedicarboxylic acid (711-02-4) → 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat (24707-07-1)

Guidance literature:

Multi-step reaction with 3 steps

1: Br₂, HgO, BrCH₂CH₂Br

2: CuO, Fe / 215 °C

3: Py

With pyridine; bromine; iron; ethylene dibromide; copper(II) oxide; mercury(II) oxide;

DOI:10.1021/ja00709a026

Reference yield:

bicyclo[2.2.2]octane-1,4-dibromide (10364-04-2) → 1,4-Bicyclo<2,2,2>oktylen-di-p-hexoxybenzoat (24707-07-1)

Guidance literature:

Multi-step reaction with 2 steps

1: CuO, Fe / 215 °C

2: Py

With pyridine; iron; copper(II) oxide;

DOI:10.1021/ja00709a026

upstream raw materials:

1,4-dihydroxybicyclo[2.2.2]octane

4-hexyloxybenzoyl chloride

1,4-bicyclo[2.2.2]octanedicarboxylic acid

bicyclo[2.2.2]octane-1,4-dibromide