C₃₃H₄₃N₃O₅SSi

Base Information

Chemical Name:C₃₃H₄₃N₃O₅SSi
CAS No.:1374110-06-1
Molecular Formula:C₃₃H₄₃N₃O₅SSi
Molecular Weight:621.873
Hs Code.:

C<sub>33</sub>H<sub>43</sub>N<sub>3</sub>O<sub>5</sub>SSi

Synonyms:C₃₃H₄₃N₃O₅SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₃N₃O₅SSi

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Technology Process of C₃₃H₄₃N₃O₅SSi

There total 5 articles about C₃₃H₄₃N₃O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1374110-05-0
C₃₃H₄₁N₃O₇SSi

: 1374110-06-1
C₃₃H₄₃N₃O₅SSi

Guidance literature:: With palladium 10% on activated carbon; ammonium formate; In tetrahydrofuran; methanol; at 20 ℃; for 27h; Inert atmosphere;

Reference yield:

: 6627-53-8
1-chloro-3-methoxy-4-nitrobenzene

: 1374110-06-1
C₃₃H₄₃N₃O₅SSi

Guidance literature:: Multi-step reaction with 5 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium acetate; tricyclohexylphosphine / 1,4-dioxane / 16 h / 90 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

3: lithium chloride; N,N,N,N,N,N-hexamethylphosphoric triamide / 16 h / 110 °C / Inert atmosphere

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice

5: ammonium formate; palladium 10% on activated carbon / methanol; tetrahydrofuran / 27 h / 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; potassium acetate; potassium carbonate; triphenylphosphine; lithium chloride; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; water;

Reference yield:

: 755026-96-1
2-(3-methoxy-4-nitrophenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1374110-06-1
C₃₃H₄₃N₃O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

2: lithium chloride; N,N,N,N,N,N-hexamethylphosphoric triamide / 16 h / 110 °C / Inert atmosphere

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 h / 20 °C / Cooling with ice

4: ammonium formate; palladium 10% on activated carbon / methanol; tetrahydrofuran / 27 h / 20 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; potassium carbonate; triphenylphosphine; lithium chloride; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water;