N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

Base Information

Chemical Name:N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester
CAS No.:438468-98-5
Molecular Formula:C₂₂H₃₅BrN₂O₇Si₂
Molecular Weight:575.604
Hs Code.:

Synonyms:N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

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Chemical Property of N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

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Technology Process of N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

There total 3 articles about N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 438468-97-4
iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

: 55715-03-2
4-bromomethyl-3-nitrobenzoic acid

: 438468-98-5
N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo020040g

Reference yield:

: 438468-96-3
N-tert-butyloxycarbonyliminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

: 438468-98-5
N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 4M HCl / dioxane / 1 h / 20 °C

2: 75 percent / DCC / CH₂Cl₂ / 0 - 20 °C

With hydrogenchloride; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jo020040g

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 438468-98-5
N-(4-(bromomethyl)-3-nitrobenzoyl)iminodiacetic acid bis[2-(trimethylsilyl)ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / DCC; DMAP / CH₂Cl₂ / 0 - 20 °C

2: 95 percent / 4M HCl / dioxane / 1 h / 20 °C

3: 75 percent / DCC / CH₂Cl₂ / 0 - 20 °C

With hydrogenchloride; dmap; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/jo020040g