N-(furan-2-ylmethyl)-3-phenylpropiolamide

Base Information

Chemical Name:N-(furan-2-ylmethyl)-3-phenylpropiolamide
CAS No.:1620886-66-9
Molecular Formula:C₁₄H₁₁NO₂
Molecular Weight:225.247
Hs Code.:

Synonyms:N-(furan-2-ylmethyl)-3-phenylpropiolamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(furan-2-ylmethyl)-3-phenylpropiolamide

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Technology Process of N-(furan-2-ylmethyl)-3-phenylpropiolamide

There total 2 articles about N-(furan-2-ylmethyl)-3-phenylpropiolamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 71189-15-6
2-(isocyanatomethyl)furan

: 536-74-3
phenylacetylene

: 1620886-66-9
N-(furan-2-ylmethyl)-3-phenylpropiolamide

Guidance literature:: phenylacetylene; With trimethylaluminum; triethylamine; In toluene; at 60 ℃; for 6h;

2-(isocyanatomethyl)furan; In toluene; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1039/d1ob01990b

Reference yield: 65.0%

: 617-89-0
furan-2-ylmethanamine

: 637-44-5
phenylpropyolic acid

: 1620886-66-9
N-(furan-2-ylmethyl)-3-phenylpropiolamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; for 6h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.8b00618

Reference yield: 78.0%

: 821-09-0
n-Pent-4-enyl alcohol

: 1620886-66-9
N-(furan-2-ylmethyl)-3-phenylpropiolamide

: 1620886-89-6
(Z)-3-chloro-N-(furan-2-ylmethyl)-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

Guidance literature:: With copper(II) chloride dihydrate; palladium diacetate; In acetonitrile; at 20 ℃; for 12h; stereoselective reaction;
DOI:10.1021/jo501317v