4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

Base Information

Chemical Name:4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane
CAS No.:110345-44-3
Molecular Formula:C₂₄H₃₈N₄O₅S₂
Molecular Weight:526.722
Hs Code.:

Synonyms:4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

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Chemical Property of 4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

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Technology Process of 4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

There total 3 articles about 4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3634-89-7
N-(p-toluenesulfonyl)aziridine

: 2620-27-1
1,5-bis(methylamino)-3-oxapentane

: 110345-44-3
4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

Guidance literature:: In acetonitrile; for 0.5h; Heating;
DOI:10.1039/b003479g

Reference yield: 62.0%

: 2620-27-1
1,5-bis(methylamino)-3-oxapentane

: 6367-75-5
2-(tosylamino)ethyl p-toluenesulfonate

: 110345-44-3
4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

Guidance literature:: With triethylamine; In acetonitrile; for 3h; Heating;
DOI:10.1007/BF00767393

Reference yield:

: 90717-00-3
2,2′-oxybis(N-tosyl-N-methylethan-1-amine)

: 110345-44-3
4,10-Dimethyl-1,13-bis(p-tolylsulfonyl)-7-oxa-1,4,10,13-tetraazatridecane

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / HBr; AcOH / 16 h / Heating

2: 98 percent / acetonitrile / 0.5 h / Heating

With hydrogen bromide; acetic acid; In acetonitrile; 2: Addition;
DOI:10.1039/b003479g