Technology Process of 2-(sulfomethyl)-3,5-dioxaheptadec-1-ene sodium salt
There total 4 articles about 2-(sulfomethyl)-3,5-dioxaheptadec-1-ene sodium salt which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate; sodium hydrogensulfite; sodium iodide;
In
water;
at 100 ℃;
for 15h;
DOI:10.1021/jo00301a048
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 56 percent / dodecyltrimethylammonium chloride / CH2Cl2 / 15 h / 30 °C
2: 77 percent / NaOH, tetrabutylammonium bisulfate / dioxane / 3 h / 60 °C
3: 74 percent / sodium sulfonate, sodium iodide, sodium carbonate, tetrabutylammonium bisulfate / H2O / 15 h / 100 °C
With
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; trimethyldodecylammonium chloride; sodium carbonate; sodium hydrogensulfite; sodium iodide;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo00301a048
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) HCl gas 2.) CaCO3 / 1.) methylene chloride, room temperature, 1 h 2.) methylene chloride, 4 h, 30 deg C
2: 56 percent / dodecyltrimethylammonium chloride / CH2Cl2 / 15 h / 30 °C
3: 77 percent / NaOH, tetrabutylammonium bisulfate / dioxane / 3 h / 60 °C
4: 74 percent / sodium sulfonate, sodium iodide, sodium carbonate, tetrabutylammonium bisulfate / H2O / 15 h / 100 °C
With
hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; trimethyldodecylammonium chloride; sodium carbonate; sodium hydrogensulfite; calcium carbonate; sodium iodide;
In
1,4-dioxane; dichloromethane; water;
DOI:10.1021/jo00301a048
