(4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate

Base Information

Chemical Name:(4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate
CAS No.:1025722-87-5
Molecular Formula:C₁₈H₂₄INO₅
Molecular Weight:461.297
Hs Code.:

Synonyms:(4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate

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Technology Process of (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate

There total 2 articles about (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1025722-84-2
(4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-5-phenyl-3-(tributylstanannyl)pent-2-enyl methyl carbonate

: 1025722-87-5
(4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate

Guidance literature:: With N-iodo-succinimide; at 0 ℃; for 0.5h;
DOI:10.1021/jo702318d

Reference yield:

: 1025722-80-8
ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-5-phenyl-3-(tributylstanannyl)pent-2-enoate

: 79-22-1
methyl chloroformate

: 1025722-87-5
(4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-3-iodo-5-phenylpent-2-enyl methyl carbonate

Guidance literature:: ethyl (4S,2E)-4-[N-(tert-butoxycarbonyl)amino]-5-phenyl-3-(tributylstanannyl)pent-2-enoate; With boron trifluoride diethyl etherate; diisobutylaluminium hydride; In dichloromethane; toluene; at 0 ℃; for 0.5h;

methyl chloroformate; With pyridine; dmap; In dichloromethane; at 0 ℃; for 1h;

With N-iodo-succinimide; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1021/jo702318d