2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

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Chemical Name:2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide
CAS No.:1437872-92-8
Molecular Formula:C₆₅H₅₅N₅O₁₁
Molecular Weight:1082.18
Hs Code.:

2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Synonyms:2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

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Chemical Property of 2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

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Technology Process of 2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

There total 18 articles about 2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1437872-95-1
2-(benzyloxy)-3-(2-methoxybenzamido)benzoic acid

: C₄₃H₃₈N₄O₇

: 1437872-92-8
2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Guidance literature:: 2-(benzyloxy)-3-(2-methoxybenzamido)benzoic acid; With thionyl chloride; for 2h; Reflux;

C₄₃H₃₈N₄O₇; With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/c3cc42349b

Reference yield:

: 90564-26-4
2-methoxy-3-nitro-benzoic acid methyl ester

: 1437872-92-8
2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / methanol; water / 2 h / Reflux

1.2: pH 1

2.1: thionyl chloride / 2 h / Reflux

3.1: iron; acetic acid / ethanol / 2 h / Reflux

4.1: thionyl chloride / 2 h / Reflux

5.1: iron; acetic acid / ethanol / 2 h / Reflux

6.1: thionyl chloride / 2 h / Reflux

With thionyl chloride; iron; acetic acid; sodium hydroxide; In methanol; ethanol; water;
DOI:10.1039/c3cc42349b

Reference yield:

: 22621-41-6
2-hydroxy-3-nitro-benzoic acid methyl ester

: 1437872-92-8
2-(benzyloxy)-3-(2-(benzyloxy)-3-(2-methoxybenzamido)benzamido)-N-(3-(3-(2-(benzyloxy)phenylcarbamoyl)-2-methoxyphenylcarbamoyl)-2-methoxyphenyl)benzamide

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 70 °C

2.1: sodium hydroxide / methanol; water / 2 h / Reflux

2.2: pH 1

3.1: thionyl chloride / 2 h / Reflux

4.1: iron; acetic acid / ethanol / 2 h / Reflux

5.1: thionyl chloride / 2 h / Reflux

6.1: iron; acetic acid / ethanol / 2 h / Reflux

7.1: thionyl chloride / 2 h / Reflux

With thionyl chloride; iron; potassium carbonate; acetic acid; sodium hydroxide; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42349b