C₄₆H₆₀Cl₃NO₁₉

Base Information

Chemical Name:C₄₆H₆₀Cl₃NO₁₉
CAS No.:192505-55-8
Molecular Formula:C₄₆H₆₀Cl₃NO₁₉
Molecular Weight:1037.34
Hs Code.:

C<sub>46</sub>H<sub>60</sub>Cl<sub>3</sub>NO<sub>19</sub>

Synonyms:C₄₆H₆₀Cl₃NO₁₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₆₀Cl₃NO₁₉

Chemical Property:

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Technology Process of C₄₆H₆₀Cl₃NO₁₉

There total 18 articles about C₄₆H₆₀Cl₃NO₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 545-06-2
trichloroacetonitrile

: (2S,3S,4S,5R,6R)-6-((2R,3R,4S,5R)-4-Acetoxy-2-acetoxymethyl-5-benzyloxy-6-hydroxy-tetrahydro-pyran-3-yloxy)-3-((2R,3S,4R,5R,6R)-6-acetoxymethyl-3,4,5-trimethoxy-tetrahydro-pyran-2-ylmethyl)-4,5-dimethoxy-tetrahydro-pyran-2-carboxylic acid benzyl ester

: 192505-55-8
C₄₆H₆₀Cl₃NO₁₉

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/S0960-894X(97)00252-7

Reference yield:

: 30694-94-1
2,4,6-tri-O-acetate-3-O-methyl-α-D-glucopyranosylbromide

: 192505-55-8
C₄₆H₆₀Cl₃NO₁₉

Guidance literature:: Multi-step reaction with 13 steps

1: 86 percent / NaBH₄ / ethanol; CH₂Cl₂ / Heating

2: 94 percent / MeONa / methanol / Ambient temperature

3: 88 percent / APTS / acetonitrile / Ambient temperature

4: 1.) BuLi, 2.) imidazole / 1.) THF, 2.) THF

5: 1.) Bu₃SnH, AIBN, 2.) 40percent aq. HF / 1.) toluene, 2.) THF

7: 86 percent / Et₃N, DMAP / CH₂Cl₂

8: 93 percent / NaH / dimethylformamide

10: 87 percent / DBU / CH₂Cl₂

11: 88 percent / TMSOTf / acetonitrile / -37 °C

12: 1.) H₂SO₄, 2.) NH₂NH₃AcO / 2.) DMF

13: 94 percent / DBU / CH₂Cl₂

With 1H-imidazole; dmap; sodium tetrahydroborate; n-butyllithium; 2,2'-azobis(isobutyronitrile); trimethylsilyl trifluoromethanesulfonate; sulfuric acid; hydrogen fluoride; tri-n-butyl-tin hydride; sodium methylate; hydrazinium monoacetate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 8-aminopyrene-1,3,6-trisulfonic acid, trisodium salt; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0960-894X(97)00252-7

Reference yield:

: 67313-50-2
1,6:2,3-dianhydro-4-O-(tetrahydropyran-2-yl)-β-D-mannopyranose

: 192505-55-8
C₄₆H₆₀Cl₃NO₁₉

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / phenylmethanol / 80 °C

2: 97 percent / DMAP, Et₃N

3: 95 percent / pTsOH / methanol / Heating

4: 88 percent / TMSOTf / acetonitrile / -37 °C

5: 1.) H₂SO₄, 2.) NH₂NH₃AcO / 2.) DMF

6: 94 percent / DBU / CH₂Cl₂

With dmap; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; hydrazinium monoacetate; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In methanol; dichloromethane; acetonitrile; benzyl alcohol;
DOI:10.1016/S0960-894X(97)00252-7