3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride

Base Information

Chemical Name:3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride
CAS No.:102618-11-1
Molecular Formula:C₁₃H₁₂N₆*ClH
Molecular Weight:288.739
Hs Code.:

Synonyms:3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride

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Chemical Property of 3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride

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Technology Process of 3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride

There total 2 articles about 3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102618-10-0
3-chloro-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine

: 102618-11-1
3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride

Guidance literature:: With hydrazine hydrate; In butan-1-ol; for 3h; Heating;
DOI:10.1002/jhet.5570220424

Reference yield:

: 84243-59-4
6-<4-(1H-imidazole-1-yl)phenyl>-3(2H)-pyridazinone

: 102618-11-1
3-hydrazino-6-<4-(1H-imidazol-1-yl)phenyl>-3(2H)-pyridazine monohydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 12 g / POCl₃ / 3 h / 90 - 92 °C

2: 1 g / N₂H₄*H₂O / butan-1-ol / 3 h / Heating

With hydrazine hydrate; trichlorophosphate; In butan-1-ol;
DOI:10.1002/jhet.5570220424