methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

Base Information

Chemical Name:methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate
CAS No.:116233-24-0
Molecular Formula:C₂₃H₂₅NO₃
Molecular Weight:363.456
Hs Code.:

Synonyms:methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

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Chemical Property of methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

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Technology Process of methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

There total 5 articles about methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 7377-26-6
4-Methoxycarbonylbenzoyl chloride

: 116233-23-9
5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthylamine

: 116233-24-0
methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

Guidance literature:: With pyridine; In benzene; Ambient temperature;
DOI:10.1021/jm00119a021

Reference yield:

: 35951-37-2
1,4-dichloro-1,4-dimethylcyclohexane

: 116233-24-0
methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 60.4 percent / AlCl₃ / 24 h / Heating

2: 86.5 percent / HNO₃, H₂SO₄ / nitromethane / 3 h / Heating

3: 84.2 percent / hydrogen / Pd/C / ethanol

4: 50 percent / pyridine / benzene / Ambient temperature

With pyridine; aluminium trichloride; sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In nitromethane; ethanol; benzene;
DOI:10.1021/jm00119a021

Reference yield:

: 67060-31-5
1,4-dimethyl-5,6-benzobicyclo<2.2.2>octane

: 116233-24-0
methyl 4-<(5,8-ethano-5,6,7,8-tetrahydro-5,8-dimethyl-2-naphthalenyl)carbamoyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 86.5 percent / HNO₃, H₂SO₄ / nitromethane / 3 h / Heating

2: 84.2 percent / hydrogen / Pd/C / ethanol

3: 50 percent / pyridine / benzene / Ambient temperature

With pyridine; sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In nitromethane; ethanol; benzene;
DOI:10.1021/jm00119a021