Technology Process of C16H18O7S
There total 4 articles about C16H18O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-(methoxycarbonyl)phenyl 3-O-prop-2-ynyl-1-thio-β-D-galactopyranoside;
With
lithium hydroxide;
In
methanol; water;
for 0.75h;
Inert atmosphere;
In
methanol; water;
Inert atmosphere;
DOI:10.1016/j.bmc.2011.03.022
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron trifluoride diethyl etherate / dichloromethane / 17 h / 20 °C / Inert atmosphere
2.1: methanol; sodium methylate / 20 °C / Inert atmosphere
3.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux; Inert atmosphere
3.2: 22 h / Reflux; Inert atmosphere
4.1: lithium hydroxide / methanol; water / 0.75 h / Inert atmosphere
4.2: amberlite IR-120 / Inert atmosphere
With
methanol; boron trifluoride diethyl etherate; sodium methylate; di(n-butyl)tin oxide; lithium hydroxide;
In
methanol; dichloromethane; water;
DOI:10.1016/j.bmc.2011.03.022
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux; Inert atmosphere
1.2: 22 h / Reflux; Inert atmosphere
2.1: lithium hydroxide / methanol; water / 0.75 h / Inert atmosphere
2.2: amberlite IR-120 / Inert atmosphere
With
di(n-butyl)tin oxide; lithium hydroxide;
In
methanol; water;
DOI:10.1016/j.bmc.2011.03.022