ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

Base Information

Chemical Name:ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate
CAS No.:110597-48-3
Molecular Formula:C₄₀H₃₄O₁₀
Molecular Weight:674.704
Hs Code.:

Synonyms:ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

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Chemical Property of ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

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Technology Process of ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

There total 6 articles about ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 7572-90-9
ethyl 2-bromo-3-(4-benzyloxy-3-methoxyphenyl)-3-oxopropionate

: 110597-47-2
3-benzyloxy-4-hydroxy-2-methoxyxanthone

: 110597-48-3
ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

Guidance literature:: With potassium tert-butylate; In acetonitrile; for 0.833333h; Ambient temperature;

Reference yield:

: 33018-29-0
4-formyl-3-hydroxy-2-methoxyxanthone

: 110597-48-3
ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / K₂CO₃ / dimethylformamide / 1 h / 140 °C

2: m-chloroperbenzoic acid / CH₂Cl₂ / 6 h / Heating

3: 10percent KOH / methanol; CHCl₃ / Heating

4: 74 percent / t-BuOK / acetonitrile / 0.83 h / Ambient temperature

With potassium hydroxide; potassium tert-butylate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 100-44-7
benzyl chloride

: 110597-48-3
ethyl 2-<9H-(3-benzyloxy-2-methoxy-9-oxo)xanthen-4-yl>oxy-3-oxo-3-(4-benzyloxy-3-methoxyphenyl)propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / K₂CO₃ / dimethylformamide / 1 h / 140 °C

2: m-chloroperbenzoic acid / CH₂Cl₂ / 6 h / Heating

3: 10percent KOH / methanol; CHCl₃ / Heating

4: 74 percent / t-BuOK / acetonitrile / 0.83 h / Ambient temperature

With potassium hydroxide; potassium tert-butylate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; acetonitrile;