6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

Base Information

Chemical Name:6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane
CAS No.:116051-30-0
Molecular Formula:C₂₀H₂₆N₂O₄
Molecular Weight:358.437
Hs Code.:

Synonyms:6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

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Chemical Property of 6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

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Technology Process of 6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

There total 18 articles about 6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

: 124339-51-1
6-<(2E)-4-keto-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

: 116051-30-0
6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 35 - 50 ℃; for 0.333333h;

Reference yield: 91.0%

: 109164-84-3
(E)-4-[2-(4-Methoxy-benzyl)-1,4-dioxo-hexahydro-pyrrolo[1,2-a]pyrazin-8a-yl]-2-methyl-but-2-enal

: 109164-86-5,116051-30-0
8a-((E)-4-Hydroxy-3-methyl-but-2-enyl)-2-(4-methoxy-benzyl)-hexahydro-pyrrolo[1,2-a]pyrazine-1,4-dione

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 40 ℃; for 0.333333h;
DOI:10.1016/S0040-4039(00)84854-6

Reference yield:

: 116005-52-8
(-)-2,5-diketo-6-(R)-allyl-4-(methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

: 116051-30-0
6-<(2E)-4-hydroxy-3-methylbut-2-enyl>-2,5-diketo-4-(4-methoxybenzyl)-1,4-diazabicyclo<4.3.0>nonane

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / O₃ / methanol

2: 2.) NaBH₄ / 2.) EtOH

With sodium tetrahydroborate; ozone; In methanol;
DOI:10.1021/ja00225a069