3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

Base Information

Chemical Name:3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide
CAS No.:1620059-12-2
Molecular Formula:C₂₃H₂₅N₇O₂S
Molecular Weight:463.563
Hs Code.:

Synonyms:3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

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Chemical Property of 3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

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Technology Process of 3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

There total 10 articles about 3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1620059-37-1
C₁₇H₁₈ClN₅

: 98-18-0
m-aminobenzenesulfonamide

: 1620059-12-2
3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

Guidance literature:: With hydrogenchloride; In ethanol; water; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.cclet.2014.06.010

Reference yield:

: 5466-43-3
2,4-dichloro-6,7-dihydro-5H-cyclopentapyrimidine

: 1620059-12-2
3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / ethanol; tetrahydrofuran / 50 h / Reflux

2: sodium hydride / 5 h / Reflux

3: hydrogenchloride / water; ethanol / 24 h / Inert atmosphere; Reflux

With hydrogenchloride; sodium hydride; sodium hydrogencarbonate; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.cclet.2014.06.010

Reference yield:

: 5466-00-2
6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diol

: 1620059-12-2
3-[[4-[N-(2,3-dimethyl-2H-indazol-6-yl)-N-methylamino]-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-yl]amino]-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 2 h / 20 °C

2: sodium hydrogencarbonate / ethanol; tetrahydrofuran / 50 h / Reflux

3: sodium hydride / 5 h / Reflux

4: hydrogenchloride / water; ethanol / 24 h / Inert atmosphere; Reflux

With hydrogenchloride; sodium hydride; sodium hydrogencarbonate; trichlorophosphate; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.cclet.2014.06.010