methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

Base Information

Chemical Name:methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate
CAS No.:1392223-07-2
Molecular Formula:C₂₄H₃₇NO₉
Molecular Weight:483.559
Hs Code.:

Synonyms:methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

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Chemical Property of methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

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Technology Process of methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

There total 3 articles about methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1392223-06-1
tert-butyl (2-(2-(2-((2-bromo-5-(methoxymethoxy)benzyl)oxy)ethoxy)ethoxy)ethyl)carbamate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1392223-07-2
methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

Guidance literature:: With potassium fluoride; palladium diacetate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 170 ℃; for 1h; Microwave irradiation;
DOI:10.1002/anie.201200867

Reference yield:

: 58402-70-3
4-bromo-1-(methoxymethoxy)-3-methylbenzene

: 1392223-07-2
methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / 95 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 0 °C

3: potassium fluoride; palladium diacetate; triethylamine; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 170 °C / Microwave irradiation

With potassium fluoride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); palladium diacetate; sodium hydride; triethylamine; triphenylphosphine; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201200867

Reference yield:

: 14472-14-1
4-bromo-3-methylphenol

: 1392223-07-2
methyl (E)-3-(2-(14,14-dimethyl-12-oxo-2,5,8,13-tetraoxa-11-azapentadecyl)-4-(methoxy-methoxy)phenyl)acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus pentoxide / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / 95 °C / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide / 0 °C

4: potassium fluoride; palladium diacetate; triethylamine; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 170 °C / Microwave irradiation

With potassium fluoride; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); phosphorus pentoxide; palladium diacetate; sodium hydride; triethylamine; triphenylphosphine; In tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.201200867