Carbamic acid, 1H-imidazol-4-yl-, 1,1-dimethylethyl ester (9CI)

Base Information

• Chemical Name: Carbamic acid, 1H-imidazol-4-yl-, 1,1-dimethylethyl ester (9CI)
• CAS No.: 34665-48-0
• Molecular Formula: C₈H₁₃N₃O₂
• Molecular Weight: 183.21
• Mol file: 34665-48-0.mol

Synonyms:Carbamic acid, 1H-imidazol-4-yl-, 1,1-dimethylethyl ester (9CI)

Chemical Property of Carbamic acid, 1H-imidazol-4-yl-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

• Boiling Point: 311.6±15.0 °C(Predicted)
• PKA: 13.03±0.70(Predicted)
• PSA: 70.50000
• Density: 1 +-.0.06 g/cm3(Predicted)
• LogP: 1.77030

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl1H-Imidazol-4-ylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamic acid, 1H-imidazol-4-yl-, 1,1-dimethylethyl ester (9CI)

There total 3 articles about Carbamic acid, 1H-imidazol-4-yl-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

1H-imidazole-4-carbonylazide (42309-94-4) + tert-butyl alcohol (75-65-0) → tert-butyl (1H-imidazol-4-yl)carbamate (34665-48-0)

Guidance literature:

for 10h; Reflux;

DOI:10.1007/s10593-021-02942-2

Reference yield:

→ tert. Butyl-imidazol-4-carbamat (34665-48-0)

Guidance literature:

Imidazol-4-carbonylazid (9), tert.-Butylalkohol;

DOI:10.1021/ja00795a026

Reference yield:

→ tert-butyl (1H-imidazol-4-yl)carbamate (34665-48-0)

Guidance literature:

Imidazol-4-carbonylazid, Curtius-Abbau;

DOI:10.1021/ja00741a048

upstream raw materials:

1H-imidazole-4-carbonylazide

tert-butyl alcohol

Downstream raw materials:

4-amino-1H-imidazole

4-aminoimidazole dihydrochloride