4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

Base Information

Chemical Name:4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile
CAS No.:154490-51-4
Molecular Formula:C₂₆H₂₅NO₅
Molecular Weight:431.488
Hs Code.:

Synonyms:4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

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Chemical Property of 4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

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Technology Process of 4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

There total 6 articles about 4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 151-50-8
potassium cyanide

: 154490-50-3
3'-benzyloxy-3,4,4'-trimethoxy-chalcone

: 154490-51-4
4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

Guidance literature:: With acetic acid; In 2-ethoxy-ethanol; at 120 ℃;
DOI:10.1016/S0040-4020(01)80559-7

Reference yield:

: 621-59-0
isovanillin

: 154490-51-4
4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 92.5 percent / potassium carbonate / dimethylformamide / 48 h / Ambient temperature

2: 92 percent / 10percent NaOH / ethanol

3: 85 percent / AcOH / 2-ethoxy-ethanol / 120 °C

With sodium hydroxide; potassium carbonate; acetic acid; In 2-ethoxy-ethanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80559-7

Reference yield:

: 100-44-7
benzyl chloride

: 154490-51-4
4-(3'-benzyloxy-4'-methoxy)phenyl-2-(3,4-dimethoxyphenyl)-4-oxobutyronitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 92.5 percent / potassium carbonate / dimethylformamide / 48 h / Ambient temperature

2: 92 percent / 10percent NaOH / ethanol

3: 85 percent / AcOH / 2-ethoxy-ethanol / 120 °C

With sodium hydroxide; potassium carbonate; acetic acid; In 2-ethoxy-ethanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)80559-7