{2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

Base Information

Chemical Name:{2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester
CAS No.:910032-87-0
Molecular Formula:C₂₃H₂₇F₃O₅
Molecular Weight:440.46
Hs Code.:

Synonyms:{2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

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Chemical Property of {2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

Chemical Property:

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Technology Process of {2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

There total 11 articles about {2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 724466-70-0
2-propyl-4-(trifluoromethyl)phenol

: 910032-81-4
[4-(3-bromo-propoxy)-2-methyl-phenoxy]-acetic acid methyl ester

: 910032-87-0
{2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/j.bmcl.2006.06.028

Reference yield:

: 944313-42-2
acetic acid 4-benzyloxy-3-methyl-phenyl ester

: 910032-87-0
{2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / sodium methanolate; MeOH / 1 h / 20 °C

2: 95 percent / aq. K₂CO₃; Bu₄NBr / Heating

3: 76 percent / H₂ / Pd/C / methanol / 20 °C / 3000.24 Torr

4: 86 percent / K₂CO₃ / acetone / Heating

5: 76 percent / K₂CO₃ / dimethylformamide / 48 h / 20 °C

With methanol; tetrabutylammomium bromide; hydrogen; sodium methylate; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; acetone; 5: Williamson reaction;
DOI:10.1016/j.bmcl.2006.06.028

Reference yield:

: 910032-98-3
1-Benzyloxy-4-(3-bromo-propoxy)-2-methyl-benzene

: 910032-87-0
{2-methyl-4-[3-(2-propyl-4-trifluoromethyl-phenoxy)-propoxy]-phenoxy}-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / H₂ / Pd/C / methanol / 20 °C / 3000.24 Torr

2: 86 percent / K₂CO₃ / acetone / Heating

3: 76 percent / K₂CO₃ / dimethylformamide / 48 h / 20 °C

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; acetone; 3: Williamson reaction;
DOI:10.1016/j.bmcl.2006.06.028