Technology Process of 9-azidononyl methanesulfonate
There total 1 articles about 9-azidononyl methanesulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / dimethyl sulfoxide / 24 h / 20 °C
2: triethylamine / dichloromethane / 24 h / 0 °C
With
sodium azide; triethylamine;
In
dichloromethane; dimethyl sulfoxide;
DOI:10.1007/s00044-014-1137-3
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutylammomium bromide; sodium hydroxide / diethyl ether; water / 72 h / 25 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Inert atmosphere; Cooling with ice
3: toluene / 22 h / Reflux
4: dichloromethane / 22 h / 25 °C
5: 2 h / 90 °C
With
lithium aluminium tetrahydride; tetrabutylammomium bromide; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; toluene;
DOI:10.1111/j.1747-0285.2011.01154.x
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutylammomium bromide; sodium hydroxide
2: lithium aluminium tetrahydride / tetrahydrofuran
3: toluene / Heating
4: dichloromethane
5: methanol / 24 h / Reflux
With
lithium aluminium tetrahydride; tetrabutylammomium bromide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1111/cbdd.12017
