Technology Process of C26H31N3O7S
There total 7 articles about C26H31N3O7S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H33N3O7S;
With
lithium hydroxide; water;
In
tetrahydrofuran;
at 20 ℃;
for 1.5h;
With
hydrogenchloride; water;
In
tetrahydrofuran;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 50 h / 20 °C
2.1: pyridine-SO3 complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3.5 h / 20 °C
3.1: Burgess Reagent / 1,2-dichloro-ethane / 0.25 h / 80 °C / Microwave
4.1: lithium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C
4.2: 20 °C
With
lithium hydroxide; 1-hydroxy-7-aza-benzotriazole; Burgess Reagent; pyridine-SO3 complex; water; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h
2.1: methanol; sodium hydroxide / tetrahydrofuran / 8 h / 0 - 20 °C
3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / DMF (N,N-dimethyl-formamide) / 50 h / 20 °C
4.1: pyridine-SO3 complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3.5 h / 20 °C
5.1: Burgess Reagent / 1,2-dichloro-ethane / 0.25 h / 80 °C / Microwave
6.1: lithium hydroxide; water / tetrahydrofuran / 1.5 h / 20 °C
6.2: 20 °C
With
methanol; lithium hydroxide; sodium hydroxide; 1-hydroxy-7-aza-benzotriazole; Burgess Reagent; pyridine-SO3 complex; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;