2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole

Base Information

• Chemical Name: 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole
• CAS No.: 1297270-52-0
• Molecular Formula: C₃₁H₂₀N₂S
• Molecular Weight: 452.579
• Mol file: 1297270-52-0.mol

Synonyms:2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole

Chemical Property of 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole

There total 3 articles about 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole (760212-40-6) + 4-dibenzothiophene boronic acid (108847-20-7) + tris-(o-tolyl)phosphine (6163-58-2) → 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole (1297270-52-0)

Guidance literature:

With potassium carbonate; palladium diacetate; In ethanol; chloroform; toluene;

Reference yield: 51.0%

2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole (760212-40-6) + 4-dibenzothiophene boronic acid (108847-20-7) → 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole (1297270-52-0)

Guidance literature:

With potassium carbonate; tris-(o-tolyl)phosphine; palladium diacetate; In water; toluene; at 80 ℃; for 6h; Inert atmosphere;

Reference yield:

4-dibenzothiophene boronic acid (108847-20-7) + tris-(o-tolyl)phosphine (6163-58-2) → 2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole (1297270-52-0)

Guidance literature:

With potassium carbonate; palladium diacetate; In 2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole; ethanol; chloroform; toluene;

upstream raw materials:

2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole

4-dibenzothiophene boronic acid

tris-(o-tolyl)phosphine