2-(3-bromophenyl)-1-phenyl-1H-benzimidazole

Base Information

• Chemical Name: 2-(3-bromophenyl)-1-phenyl-1H-benzimidazole
• CAS No.: 760212-40-6
• Molecular Formula: C19H13BrN2
• Molecular Weight: 349.23
• Hs Code.: 2933290090
• Mol file: 760212-40-6.mol

Synonyms:2-(3-Bromophenyl)-1-phenyl-1H-benzimidazole;1-Phenyl-2-(3-bromophenyl)benzimidazole;2-(3-Bromophenyl)-1-phenylbenzimidazole;

Chemical Property of 2-(3-bromophenyl)-1-phenyl-1H-benzimidazole

Chemical Property:

• Vapor Pressure: 1.17E-10mmHg at 25°C
• Melting Point: 123.0 to 127.0 °C
• Refractive Index: 1.671
• Boiling Point: 513.6 °C at 760 mmHg
• Flash Point: 264.4 °C
• PSA: 17.82000
• Density: 1.38 g/cm³
• LogP: 5.45500
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

2-(3-Bromophenyl)-1-phenyl-1H-benzo[d]imidazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(3-bromophenyl)-1-phenyl-1H-benzimidazole

There total 8 articles about 2-(3-bromophenyl)-1-phenyl-1H-benzimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-bromobenzoyl chloride (1711-09-7) + N-phenyl-1,2-benzenediamine (534-85-0) → 2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole (760212-40-6)

Guidance literature:

3-bromobenzoyl chloride; N-phenyl-1,2-benzenediamine; With triethylamine; In dichloromethane; at 20 ℃; for 23h;

With trichlorophosphate; In 1,4-dioxane; at 75 - 115 ℃; for 2h;

Reference yield: 96.0%

3-bromobenzoyl chloride (1711-09-7) + N-phenyl-o-phenylene-1,2-diamine → 2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole (760212-40-6)

Guidance literature:

With triethylamine; trichlorophosphate; In 1,4-dioxane; dichloromethane; water;

Reference yield: 86.0%

m-bromobenzoic aldehyde (3132-99-8) + N-phenyl-1,2-benzenediamine (534-85-0) → 2-2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole (760212-40-6)

Guidance literature:

With sodium metabisulfite; In N,N-dimethyl-formamide; at 100 ℃; for 0.1h; Microwave irradiation;

DOI:10.1002/jhet.1058

upstream raw materials:

3-bromobenzoyl chloride

N-phenyl-1,2-benzenediamine

C₁₉H₁₅BrN₂O

m-bromobenzoic aldehyde

Downstream raw materials:

1-phenyl-2-(3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1H-benzo[d]imidazole

C₅₇H₃₉N₅

2-[3-(dibenzothiophen-4-yl)phenyl]-1-phenyl-1H-benzimidazole

9-(3-(1-phenyl-1H-benzo[d]imidazol-2-yl)phenyl)-9H-carbazole