1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene

Base Information

Chemical Name:1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene
CAS No.:1402168-11-9
Molecular Formula:C₄₆H₃₄Br₂N₆O₂S₂
Molecular Weight:926.755
Hs Code.:

Synonyms:1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene

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Chemical Property of 1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene

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Technology Process of 1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene

There total 2 articles about 1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 123692-94-4
2-hydroxy-5-((4-bromophenyl)diazenyl)benzaldehyde

: 152367-75-4
2-[(2-[[(2-aminophenyl)sulfanyl]methyl]benzyl)sulfanyl]aniline

: 1402168-11-9
1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene

Guidance literature:: In ethanol; at 60 - 80 ℃; for 4h;
DOI:10.1016/j.saa.2012.07.013

Reference yield:

: 90-02-8
salicylaldehyde

: 127125-47-7
C₆H₄BrClN₂

: 1402168-11-9
1,2-bis(4-((4-bromophenyl)diazenyl)-2-((2-(methylthio)phenylimino)methyl)phenol)methylenbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / water / 0.5 h / 0 °C

1.2: 1 h / 0 - 5 °C

2.1: ethanol / 4 h / 60 - 80 °C

With sodium hydroxide; In ethanol; water;
DOI:10.1016/j.saa.2012.07.013