ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

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Chemical Name:ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate
CAS No.:1407969-12-3
Molecular Formula:C₈₂H₁₀₄O₆Si₂
Molecular Weight:1241.9
Hs Code.:

ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

Synonyms:ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

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Chemical Property of ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

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Technology Process of ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

There total 2 articles about ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 41302-32-3
ethyl 5-iodopentanoate

: 1407968-97-1
2-(3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-5-tert-butyl-2-hydroxybenzyl)-6-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-4-tert-butylphenol

: 1407969-12-3
ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

Guidance literature:: With potassium carbonate; In acetonitrile; for 9h; Reflux;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 992-52-9
2-<3-<3-(5-tert-Butylsalicyl)-5-tert-butylsalicyl>-5-tert-butylsalicyl>-4-tert-butylphenol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1407969-12-3
ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-3-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-2-hydroxybenzyl)phenoxy)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 20 °C / Inert atmosphere

2: potassium carbonate / acetonitrile / 9 h / Reflux

With 1H-imidazole; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.09.032