C₂₈H₄₈O₄Si

Base Information

Chemical Name:C₂₈H₄₈O₄Si
CAS No.:1380242-30-7
Molecular Formula:C₂₈H₄₈O₄Si
Molecular Weight:476.772
Hs Code.:

C<sub>28</sub>H<sub>48</sub>O<sub>4</sub>Si

Synonyms:C₂₈H₄₈O₄Si

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Chemical Property of C₂₈H₄₈O₄Si

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Technology Process of C₂₈H₄₈O₄Si

There total 8 articles about C₂₈H₄₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1380242-19-2
C₂₅H₄₄O₄Si

: 77-76-9
2,2-dimethoxy-propane

: 1380242-30-7
C₂₈H₄₈O₄Si

Guidance literature:: With toluene-4-sulfonic acid; In acetone; at 20 ℃; for 16h;
DOI:10.1002/anie.201201395

Reference yield:

: 1380242-16-9
C₃₁H₄₅NO₄SSi

: 1380242-30-7
C₂₈H₄₈O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 3 h / -78 °C / Inert atmosphere

2.1: titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / -78 °C / Inert atmosphere

3.1: trimethylaluminum / dichloromethane; toluene / 0.5 h / -10 - 20 °C / Inert atmosphere

3.2: 8 h / -10 °C / Inert atmosphere

4.1: methyllithium / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

4.2: 2 h / -78 °C / Inert atmosphere

5.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 17 h / -30 - -15 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / acetone / 16 h / 20 °C

With tetramethylammonium triacetoxyborohydride; methyllithium; trimethylaluminum; titanium tetrachloride; diisobutylaluminium hydride; toluene-4-sulfonic acid; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; dichloromethane; cyclohexane; acetone; toluene; acetonitrile;
DOI:10.1002/anie.201201395

Reference yield:

: 1380242-18-1
C₂₉H₄₉NO₅SSi

: 1380242-30-7
C₂₈H₄₈O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: trimethylaluminum / dichloromethane; toluene / 0.5 h / -10 - 20 °C / Inert atmosphere

1.2: 8 h / -10 °C / Inert atmosphere

2.1: methyllithium / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

2.2: 2 h / -78 °C / Inert atmosphere

3.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 17 h / -30 - -15 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / acetone / 16 h / 20 °C

With tetramethylammonium triacetoxyborohydride; methyllithium; trimethylaluminum; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene; acetonitrile;
DOI:10.1002/anie.201201395