(+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane

Base Information

• Chemical Name: (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane
• CAS No.: 1089140-12-4
• Molecular Formula: C₂₀H₁₈N₈O₂
• Molecular Weight: 402.415
• Mol file: 1089140-12-4.mol

Synonyms:(+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane

Chemical Property of (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane

There total 1 articles about (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

N,N'-bis(benzyliden)ethylendiamine (104-71-2) + azidoacetic acid potassium salt → (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane (1089140-12-4) + (+/-)-1,2-bis[3'-azido-4'-phenylazetidin-2'-one-1'-yl]ethane

Guidance literature:

With bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; at 0 - 25 ℃;

DOI:10.1039/b809221d

Reference yield:

(4R)-N-(prop-2-yn-1-yl)-4-((3R,7R,10S,12S,13R)-3,7,12-trihydroxy-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanamide (1021182-35-3) + (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane (1089140-12-4) → C74H104N10O10 (1091597-14-6)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; for 0.0833333h; Microwave irradiation;

DOI:10.1039/b809221d

Reference yield:

propargyl 3α,12α-dihydroxy-5β-cholan-24-oate (868595-03-3) + (+/-)-1-[3'-azido-4'-phenylazetidin-2'-one-1'-yl]-2-[3''-azido-4''-phenyl-azetidin-2''-one-1''-yl]ethane (1089140-12-4) → C74H102N8O10 (1091597-12-4)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; for 0.0833333h; Microwave irradiation;

DOI:10.1039/b809221d

upstream raw materials:

N,N'-bis(benzyliden)ethylendiamine

Downstream raw materials:

C₇₄H₁₀₂N₈O₁₀

C₇₄H₁₀₂N₈O₁₂

C₇₄H₁₀₄N₁₀O₁₀

C₇₄H₁₀₄N₁₀O₈