(E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

Base Information

Chemical Name:(E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal
CAS No.:911125-73-0
Molecular Formula:C₂₈H₃₀O₅
Molecular Weight:446.543
Hs Code.:

Synonyms:(E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

Chemical Property:

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Technology Process of (E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

There total 3 articles about (E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66958-67-6
1,4-bis(benzyloxy)-2,3-dimethoxy-5-methyl-6-(3-methylbut-2-enyl)benzene

: 911125-73-0
(E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

Guidance literature:: With selenium(IV) oxide; In ethanol; for 2h; Heating;
DOI:10.1002/hlca.200690130

Reference yield:

: 727-81-1
2,3-dimethoxy-5-methyl-6-(3-methyl-2-butenyl)-1,4-benzoquinone

: 911125-73-0
(E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

Guidance literature:: Multi-step reaction with 3 steps

1: aq. Na₂S₂O₄ / methanol / 3 h / 20 °C

2: 12.36 g / KOH; Bu₄NBr / acetone / 3 h / 20 °C / Heating

3: SeO₂ / ethanol / 2 h / Heating

With potassium hydroxide; selenium(IV) oxide; sodium dithionite; tetrabutylammomium bromide; In methanol; ethanol; acetone;
DOI:10.1002/hlca.200690130

Reference yield:

: 52590-98-4
1-ubiquinol

: 911125-73-0
(E)-4-(2,5-Bis-benzyloxy-3,4-dimethoxy-6-methyl-phenyl)-2-methyl-but-2-enal

Guidance literature:: Multi-step reaction with 2 steps

1: 12.36 g / KOH; Bu₄NBr / acetone / 3 h / 20 °C / Heating

2: SeO₂ / ethanol / 2 h / Heating

With potassium hydroxide; selenium(IV) oxide; tetrabutylammomium bromide; In ethanol; acetone;
DOI:10.1002/hlca.200690130